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In our previous work [2] nPd0(Hx2n)MoO3/C electrodes were prepared by reaction of Pd(II) salts and reduced forms of hydrogen-containing molybdenum bronzes under open-circuit conditions. These electrodes demonstrated the high activity towards the reactions of carbon monoxide and methanol electrooxidation. In present work the deposition of palladium were performed at the surface of previously reduced hydrogen containing molybdenum bronzes (HxMoO3).