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Modern technology of organic semiconductor structures is in permanent search for new and promising materials. The emergence of hybrid materials (HM) has become a natural development of this industry. Such substances not only combine the best features of organic and inorganic components, but also exhibit interesting properties under the action of laser radiation. In this research, thin films of HM based on tris-(8-hydroxyquinoline)gallium (Gaq3) were fabricated. The exchange reaction between the components was initiated by laser radiation, causing the changes of optical properties.