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This report is aimed at synthesizing new highly efficient single crystals and glass-crystalline nano-structures from multicomponent oxide melts tending to form a wide variety of phases exhibiting diverse compositions and structures that, for a number of reasons, are not realized in nature. This work is mainly focused on studying the crystal genesis in borate systems pursuing optimization of growth conditions for (Er,Yb):RAl3(BO3)4 (R=Y or lanthanide) single crystals and fabrication of glass-crystalline nano-composites.