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The properties of a number of low-melting lead fluoroborate, bo-rosilicate and fluoroborosilicate glasses evaluated for the synthesis of luminescent hybrid materials. Hybrid materials with -diketone com-plexes of lanthanides were synthesized on the basis of the selected glasses. The effect of exposure to air, heating, and partial crystallization of the glass matrix on the stability of the spectral-luminescent properties of hybrid materials was investigated.