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The synthesis and properties of several new energetic derivatives of 1,2,4-triazolo[4,3-b][1,2,4,5]tetrazine are described. These are energetic salts of 3-nitroguanidine-1,2,4-triazolo[4,3-b][1,2,4,5]tetrazine, 6-methyl-3-nitroguanidine-1,2,4-triazolo[4,3-b][1,2,4,5]-tetrazine and 3-guanidino-1,2,4-triazolo[4,3-b][1,2,4,5]tetrazine. All the synthesized derivatives of 3-guanidino-1,2,4-triazolo[4,3-b][1,2,4,5]tetrazine were identified by FTIR, 1H, 13C NMR spectroscopy, LCMS and elemental analyses.