Evaluation of thermal analysis experimental data II. Optimal conditions for evolved gas analysis of thermal decomposition of solidsстатья
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Дата последнего поиска статьи во внешних источниках: 12 октября 2013 г.
Аннотация:The influence of various factors on EGA and TG/DTG results of thermal decomposition of solids is analyzed. Following factors have been considered: the flow rate of the gas medium in the dynamic measurements, the diffusion resistance of the solid sample for gaseous products, the shape of samples, the grain size distribution of the disperse samples. The ways how to determine optimum values of the parameter have been discussed. The use of THERMOKIN software package is recommended for this purpose.