Аннотация:Powder hybrid materials based on the organic phosphor 8-hydroxyquinolate lithium and the inorganic matrix PbF2 have been synthesized. Powder hybrid materials were obtained by coprecipitation from aqueous-alcoholic solutions with ammonium fluoride under various conditions - different concentrations of the organic component, precursor solutions, and the order of mixing the reagents. The resulting hybrid materials showed effective broadband luminescence in the 390-700 nm. In all obtained hybrid materials, a shift of the photoluminescence bands is observed, which is characteristic of the formation of lead luminescent complexes. The conditions for obtaining the most intense luminescence are determined.