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Synthesis of energetic compounds from 5-azido-2,2-dimethyl-5-nitro-1,3-dioxaneстатья
- Авторы: Rudakov G.F., Katorov D.V., Simonov D.P., Dubovis M.V., Zhilin V.F.
- Сборник: Proceedings of the 12th Seminar of the New Trends in Research of Energetic Materials (NTREM)
- Том: 2
- Год издания: 2009
- Место издания: University of Pardubice Czech Republic
- Первая страница: 793
- Последняя страница: 797
- Аннотация: The synthesis of 1,2,3-triazoles via 1,3-dipolar cycloaddition of 5-azido-2,2-dimethyl-5-nitro-1,3-dioxane to propargyl alcohol and 2-butyne-1,4-diol is reported. New azidomethyl- and nitroxymethyl-1,2,3-triazole derivatives have been synthesized as products of this addition. The synthesized 1,2,3-triazoles have been identified by means of IR, NMR spectral and elemental analyses. Thermal behavior of new compounds has been studied by means of TGA/DTA analysis.
- Добавил в систему: Рудаков Геннадий Федорович